Structural and Surface Analysis

Structural and surface analysis enables the high-resolution characterization of particles, fibers, biomaterials, and functional surfaces. By combining microscopic and spectroscopic techniques, morphology, material composition, and chemical properties can be comprehensively investigated.

Application Areas

  • Polymer, fiber, and membrane materials
  • Medical devices and functional surfaces
  • Characterization of new materials and formulations
  • Aging, damage, and failure analysis
  • Process-related research and development

Scanning Electron Microscopy (SEM)

Agglomeration and Dispersion States of Polymer Microparticles. (Scale bar 100 µm)
Morphology of polymer nanofibers.
(Scale bar: 2 µm)
Morphology of gold nanoparticles.
(Scale bar: 1 µm)

Scanning electron microscopy (SEM) enables high-resolution investigation of surface structures, morphologies, and material properties in the micro- and nanometer range. 

The detailed visualization of particles, fibers, layers, and surfaces allows structure–property relationships to be analyzed and supports development, optimization, and failure analysis processes.

  • Investigation of morphology and surface structure
  • Determination of particle shape and size distribution
  • Analysis of agglomeration and dispersion states
  • Characterization of surface roughness and defects
  • Investigation of foreign particles
  • Comparative analysis of materials and manufacturing processes

 

Sample Requirements

Sample requirements depend on the material properties and the objective of the analysis. Suitable sample types include, for example, powders, particles, fibers, coatings, biomaterials, and solid surfaces. Nanomaterials can be deposited from dispersions onto suitable substrates. If required, non-conductive samples are coated with a thin conductive layer prior to measurement.

 

Elemental Analysis (EDX)

In addition to SEM imaging, energy-dispersive X-ray spectroscopy (EDX) can be used to analyze the elemental composition and distribution of inorganic constituents.

  • Qualitative and semiquantitative elemental analysis
  • Elemental distribution analysis (mapping, line scans, and point analyses)
  • Identification of inorganic constituents and contaminants

Raman Microscopy

Raman microscopy enables minimally destructive chemical characterization of materials with high spatial resolution. By analyzing molecular-specific vibrational modes, materials can be identified, chemical differences can be visualized, and the distribution of components within complex samples can be investigated.

  • Identification of polymers, biomaterials, and particles
  • Chemical characterization of surfaces and coatings
  • Spatially resolved analysis of material distributions (Raman mapping)